The distillation column is an important processing unit in the chemical and oil refining industry. Distillation is the most widely employed separation method in the world’s oil plants, chemical and petrochemical industrial facilities. The main drawback of the technique is high energy consumption, which leads to high production costs. Therefore, distillation columns are required to be controlled close to the desired steady state conditions because of economic incentives. Most industrial distillation columns are currently controlled by conventional multi-loop controllers such as proportional-integral-derivative (PID) controllers, which have several shortcomings such as difficulty coping with sudden set-point jumps, complications due to the integral term (I), and performance degradation due to the effect of noise on the derivative term (D). The control of ill-conditioned and strongly non-linear plants such as high purity distillation needs advanced control schemes for high control performance. This thesis investigates the use of active disturbance rejection control (ADRC) for product composition control in distillation columns. To the author’s knowledge, there are few reported applications of ADRC in the chemical industry. Most ADRC applications are in electrical, robotics and others. Therefore, this research will be the first to apply the ADRC scheme in a common chemical processing unit, and can be considered as a first contribution of this research. Initially, both PI and ADRC schemes are developed and implemented on the Wood–Berry distillation column transfer function model, on a simulated binary distillation column based on a detailed mechanistic model, and on a simulated heat integrated distillation column (HIDiC) based on a detailed mechanistic model. Process reaction curve method and system identification tools are used to obtain the 2×2 multi-input multi-output (MIMO) transfer function of both binary and HIDiC for the purpose of PI tuning where the biggest log-modulus tuning (BLT) method is used. Then, the control performance of ADRC is compared to that of the traditional PI control in terms of set-point tracking and disturbance rejection. The simulation result clearly indicates that the ADRC gives better control performance than PI control in all three case studies.

The distillation column is an important processing unit in the chemical and oil refining industry. Distillation is the most widely employed separation method in the world’s oil plants, chemical and petrochemical industrial facilities. The main drawback of the technique is high energy consumption, w...